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1H-NMR spectra of all diastereomeric nitroalditols with a chain length up to C7, obtained from aldoses by the Fischer-Sowden reaction

✍ Scribed by Köll, Peter ;Brandenburg, Heinz ;Seelhorst, Willi ;Stenns, Claudia ;Kogelberg, Heide


Publisher
John Wiley and Sons
Year
1991
Tongue
English
Weight
406 KB
Volume
1991
Category
Article
ISSN
0947-3440

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✦ Synopsis


Abstract

The ^1^H‐NMR spectra of all diastereomeric alditols with a terminal nitro group up to a chain length of seven carbon atoms (31 compounds) have been recorded at 500 MHz in D~2~O. In most cases, a complete first‐order analysis has been performed. The spectra show systematic correlations with those of the parent alditols. Despite a special situation around the nitromethyl group no severe deviations of preferred conformations in solution from those of the parent alditols have been observed.