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1H n.m.r. spectra and ensuing conformational evidence on carbon–carbon double bonded systems. (Electrically neutral organic Lewis acids—33)

✍ Scribed by E. Haslinger; P. Wolschann


Publisher
John Wiley and Sons
Year
1977
Tongue
English
Weight
599 KB
Volume
9
Category
Article
ISSN
0749-1581

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✦ Synopsis


Abstract

The n.m.r. spectra of various derivatives of the cyclic acylal of malonic acid and of dimethylbarbituric acid are described. From the long range coupling constant, conformational evidence on the dihedral angle θ between the aromatic ring and the diketodioxane ring or the N,N‐dimethylbarbituric acid ring can be derived. The investigated substances show a dependence of θ on the aromatic substitution.