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1H NMR separation of epimeric mixtures by lanthanide shift reagents: Analysis of some isoxazolidine derivatives

✍ Scribed by P. Bucci; G. Chidichimo; A. Liguori; G. Menniti; N. Uccella

Publisher: John Wiley and Sons
Year: 1984
Tongue: English
Weight: 300 KB
Volume: 22
Category: Article
ISSN: 0749-1581
DOI: 10.1002/mrc.1270220611

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✦ Synopsis

Epimeric mixtures of isoHazolidine derivatives were investigated by ' H NMR spectra obtained in the presence of lanthanide shift reagents. The NMR signals of all the components contained in a mixture of 2 , 3 -d i p n e n y l -S -c e ~y ~~~~e s were identified and the LISCA computer program enabled the stereochemistry of the Merent isomers to be established.

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