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1H and 13C nuclear magnetic resonance study of (D3)-trishomocuban-4-ol and (D3)-trishomocubanone

✍ Scribed by Theodor G. Dekker; Douglas W. Oliver; Klaus G. R. Pachler; Philippus L. Wessels; Marianne Woudenberg

Publisher
John Wiley and Sons
Year
1981
Tongue
English
Weight
530 KB
Volume
15
Category
Article
ISSN
0749-1581

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✦ Synopsis

Abstract

The complete assignments of the ^1^H and ^13^C NMR spectra for (D~3~)‐trishomocuban‐4‐ol (3) and (D~3~)‐trishomocubanone (4) are reported. The difference between the ^1^H and ^13^C chemical shifts of 3 and 4 and those of the hydrocarbon (D~3~)‐trishomocubane, and the substituent effect of the hydroxy group, can be adequately explained by the unique stereochemistry of these compounds.

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