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1H and 13C n.m.r. study of butatriene-bis-tricarbonyliron complexes. Assignment of geometric orientation by comparative J(CCCH) values

✍ Scribed by Rae Victor; Israel Ringel


Publisher
John Wiley and Sons
Year
1978
Tongue
English
Weight
281 KB
Volume
11
Category
Article
ISSN
0749-1581

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✦ Synopsis


Abstract

A number of substituted butatriene‐bis‐tricarbonyliron complexes have been studied by ^13^C and ^1^H n.m.r. spectroscopy. Long range coupling values, J(CCCH), have confirmed chemical shift results that methyl and phenyl groups assume opposite orientations at the coordinated double bonds with the methyl group preferentially trans to carbon and the phenyl group preferentially trans to iron.