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1H and 13C NMR Spectroscopy analysis of acetonides of D-Glucitol Derivatives

✍ Scribed by Lucilia Kato; Raquel Marques Braga

Publisher: John Wiley and Sons
Year: 1999
Tongue: English
Weight: 52 KB
Volume: 37
Category: Article
ISSN: 0749-1581
DOI: 10.1002/(sici)1097-458x(199906)37:6<447::aid-mrc476>3.0.co;2-l

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✦ Synopsis

A series of acetonides was obtained during the formal synthesis of deoxynojirimycin. The 1 H NMR spectra of these derivatives contain strongly coupled multiplets covering a chemical shift range of about 1 ppm. The spectra are severely complicated by second-order effects and were assigned by 2D NMR and 13 C NMR experiments.

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