## Abstract The ^1^H and ^13^C NMR spectra of the two phytohormones, brassinolide and 24‐epi‐brassinolide, and the two synthetic analogues 22,23,24‐trisepi‐brassinolide and (22__S__,23__S__)‐28‐homo‐brassinolide, were assigned using 1D and 2D NMR techniques. Independent assignment strategies are pr
1H and 13C NMR analysis of three quinone-methide triterpenoids
✍ Scribed by A. A. Leslie Gunatilaka; H. Chandrasiri Fernando; Tohru Kikuchi; Yasuhiro Tezuka
- Publisher
- John Wiley and Sons
- Year
- 1989
- Tongue
- English
- Weight
- 311 KB
- Volume
- 27
- Category
- Article
- ISSN
- 0749-1581
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✦ Synopsis
Detailed analysis of the 'H and 13C NMR spectra of three natural quinone-methide triterpenoids, pristimerin, tingenone and 20-hydroxytingenone, was carried out by the application of two-dimensional H-'H and ' H-13C shift correlation techniques. Some previous 'H and "C assignments have been revised. KEYWORDS 'H NMR l3C NMR Quinone-methide triterpenoids Revised assignments
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