𝔖 Bobbio Scriptorium
✦   LIBER   ✦

1H and 13C NMR analysis of three quinone-methide triterpenoids

✍ Scribed by A. A. Leslie Gunatilaka; H. Chandrasiri Fernando; Tohru Kikuchi; Yasuhiro Tezuka


Publisher
John Wiley and Sons
Year
1989
Tongue
English
Weight
311 KB
Volume
27
Category
Article
ISSN
0749-1581

No coin nor oath required. For personal study only.

✦ Synopsis


Detailed analysis of the 'H and 13C NMR spectra of three natural quinone-methide triterpenoids, pristimerin, tingenone and 20-hydroxytingenone, was carried out by the application of two-dimensional H-'H and ' H-13C shift correlation techniques. Some previous 'H and "C assignments have been revised. KEYWORDS 'H NMR l3C NMR Quinone-methide triterpenoids Revised assignments


📜 SIMILAR VOLUMES


1H and 13C NMR analysis of brassinostero
✍ Andrea Porzel; Volker Marquardt; Günter Adam; Georges Massiot; Dieter Zeigan 📂 Article 📅 1992 🏛 John Wiley and Sons 🌐 English ⚖ 408 KB

## Abstract The ^1^H and ^13^C NMR spectra of the two phytohormones, brassinolide and 24‐epi‐brassinolide, and the two synthetic analogues 22,23,24‐trisepi‐brassinolide and (22__S__,23__S__)‐28‐homo‐brassinolide, were assigned using 1D and 2D NMR techniques. Independent assignment strategies are pr

Total assignment of 1H and 13C NMR spect
✍ F. J. Q. Monte; J. P. Kintzinger; R. Braz-Filho 📂 Article 📅 1997 🏛 John Wiley and Sons 🌐 English ⚖ 204 KB 👁 2 views

The complete 1H and 13C assignment of two closely related isomeric triterpenoid derivatives (methyl 2a,3b-di-Oacetylolean-12-en-28-oate and methyl 2a,3a-di-O-acetylurs-12-en-28-oate) is described. In addition to 1D NMR methods, 2D shift-correlated NMR techniques (COSY, NOESY, HMBC and HMQC) were use

Structural and 1H and 13C NMR analysis o
✍ Wayne W. Harding; Helen Jacobs; Stewart McLean; William F. Reynolds 📂 Article 📅 2001 🏛 John Wiley and Sons 🌐 English ⚖ 97 KB

## Abstract The ^1^H and ^13^C NMR spectra of the glabretal derivatives, 21,24‐epoxy‐3α, 7α, 21,23‐tetraacetoxy‐25‐hydroxy‐4α,4β,8β‐trimethyl‐14,18‐cyclo‐5α,13α,14α,17α‐cholestane and 21,23‐epoxy‐3α,7α,21,24,25‐pentaacetoxy‐4α,4β,8β‐trimethyl‐14,18‐cyclo‐5α,13α,14α,17α‐cholestane, obtained from an

Total assignment of 1H and 13C NMR spect
✍ F. J. Q. Monte; S. M. A. Papa; J. P. Kintzinger; R. Braz-Filho 📂 Article 📅 2000 🏛 John Wiley and Sons 🌐 English ⚖ 55 KB 👁 2 views

The complete 1 H and 13 C chemical shift assignment of two closely related isomeric triterpenoids, 3˛,16˛,20(R),25-tetrahydroxy-2,11,22-trioxocucurbita-5,23(E)-diene and 3ˇ,16˛,20(R)-trihydroxy-25-acetoxy-2,11,22trioxocucurbita-5,23(E)-diene, making use of one-and two-dimensional NMR techniques (HMB

1H and 13C NMR spectral assignments of f
✍ Juliana de Brito Cysne; Raimundo Braz-Filho; Marcus Vinícius Assunção; Daniel E. 📂 Article 📅 2006 🏛 John Wiley and Sons 🌐 English ⚖ 123 KB

## Abstract The phytochemical investigation of carnauba wax led to the isolation of three new dammarane triterpenoids 1, 2 and 4, together with the known triterpene 3. The structures of the new compounds were determined by 1D and 2D NMR spectroscopy and by comparison with published data for closely

1H and 13C NMR assignments for four trit
✍ Li-Feng Han; Bai-Ping Ma; Hong-Sheng Zhang; Xin-Bo Song; Xiu-Mei Gao; Li-Ping Ka 📂 Article 📅 2008 🏛 John Wiley and Sons 🌐 English ⚖ 139 KB 👁 1 views

## Abstract Four triterpenoid saponins were isolated from Albizziae cortex, and a complete assignment of their ^1^H and ^13^C NMR spectra was carried out using 1D and 2D NMR (^1^H^1^H COSY, HSQC, HMBC, and HSQC–TOCSY) methods. Their ^1^H NMR assignments were reported for the first time and some of