## Abstract Analyses of the ^1^H, ^13^C and ^19^F NMR spectra of 15 mono‐, di‐, tri‐ or tetrafluoro‐substituted steroids were carried out by two‐dimensional ^1^H^1^H and ^1^H^13^C shift correlation experiments.
1H, 13C and 19F NMR studies on fluorinated ethers
✍ Scribed by P.E. Balonga; V.J. Kowalewski; R.H. Contreras
- Publisher
- Elsevier Science
- Year
- 1988
- Tongue
- English
- Weight
- 336 KB
- Volume
- 44
- Category
- Article
- ISSN
- 1386-1425
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✦ Synopsis
The enflurane and ethoxyflurane 'H, 13C and 19F NMR spectrd are examined-including sign determmatlon of F-F and F-H couphngs-and considered 1n the hght of previously reported results for methoxyflurane Conformat1onal differences between methoxyflurane and the former two molecules dre indicated by through space F-H coupling constants and by the nonequivalence of gem1ndl fluorine nuclei Populations of conformers about the C-C bond dre estimated
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