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1,6,7,7-Tetrachloro-5-methyl-2-phenyl-3-azabicyclo[4.1.0]heptan-4-one

✍ Scribed by Tinant, B. ;Declercq, J. P. ;Rouchy, P. ;Guillot, N.

Book ID
114508338
Publisher
International Union of Crystallography
Year
1991
Tongue
English
Weight
202 KB
Volume
47
Category
Article
ISSN
0108-2701

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The title compound, C 18 H 20 ClNO 2 , has been synthesized by the reaction of 4-chlorobenzaldehyde, Meldrum's acid, dimedone and CH 3 NH 3 Cl(NaOAc) in ethanol under microwave irradiation. The pyridone ring adopts a screw-boat conformation and the cyclohexenone ring an envelope conformation.