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16-Substituted Steroids. XVIII. 1 6,16-Difunctional 3,5-Cyclo-5α-androstanes

✍ Scribed by Rhone, James R.; Huffman, Max N.; Stanley, Allan J.

Book ID
126179743
Publisher
American Chemical Society
Year
1962
Tongue
English
Weight
300 KB
Volume
5
Category
Article
ISSN
0022-2623

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✍ James R. Rhone; Max N. Huffman 📂 Article 📅 1965 🏛 Elsevier Science 🌐 French ⚖ 145 KB

Contrary to a report (1) in the literature that estrone-16 (16-keto-estra-1,3,5(10)-trien-3-01) (2) fails to form an enol acetate, we have found that, with the aid of anhydrous E-toluenesulfonic acid as a catalyst, estra-1,3,5(1C),16-tetraene-3, 16-diol diacetate can be successfully obtained in stab