✦ LIBER ✦
1,6-Methano[10]annulene has a Delocalized Structure in S0 and S1: High-Resolution Spectroscopy in a Supersonic Jet
✍ Scribed by Reinhold Seiler; Bernhard Dick
- Publisher
- John Wiley and Sons
- Year
- 2001
- Tongue
- English
- Weight
- 84 KB
- Volume
- 40
- Category
- Article
- ISSN
- 0044-8249
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✦ Synopsis
The synthesis of the potassium salt was analogous to that of the compound 2, with a stoichiometric amount of potassium hydroxide instead of tetra-n-butylammonium hydroxide. Green crystals were isolated by filtering immediately after cooling the autoclave to room temperature. Yield (based on the solvent free compound): 0.36 g (0.084 mmol), 41 %. Elemental analysis calcd (%, based on the solvent free compound) for