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1,6-Dimethyl-1α,4α,4aα,5α,8β,8aα-hexahydro-1,4-methanonaphthalene-5,8-diol

✍ Scribed by Flippen-Anderson, J. L. ;Gilardi, R. ;George, C. ;Marchand, A. P. ;Jin, P. w.

Book ID
114504444
Publisher
International Union of Crystallography
Year
1987
Tongue
English
Weight
328 KB
Volume
43
Category
Article
ISSN
0108-2701

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## Abstract Diels–Alder cycloaddition of a mixture of 1‐ and 2‐methylcyclopentadienes (1a and 1b, respectively) to 2‐methoxy‐__p__‐benzoquinone (2) gave a mixture of isomeric __endo__ [4 + 2] cycloadducts (3a–3d). Fractional recrystallization of this product mixture from EtOAc‐hexane gave 6‐methoxy