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1,4,5,8-Tetrakis(dimethylamino)naphthalene: Synthesis, Structure, “Proton Sponge” and Electron Donor Properties

✍ Scribed by Dipl.-Chem. Thomas Barth; Claus Krieger; Prof. Dr. Franz A. Neugebauer; Prof. Dr. Heinz A. Staab

Publisher
John Wiley and Sons
Year
1991
Tongue
English
Weight
320 KB
Volume
30
Category
Article
ISSN
0044-8249

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Low-temperature (120 K) structure and vi
Low-temperature (120 K) structure and vibrational spectrum of protonated proton sponge: the adduct of 1,8-bis(dimethylamino)naphthalene (DMAN) with 4,5- dicyanoimidazole (DCI)
✍ Eugeniusz Grech; Zbigniew Malarski; Wanda Sawka-Dobrowolska; Lucjan Sobczyk 📂 Article 📅 1999 🏛 John Wiley and Sons 🌐 English ⚖ 111 KB 👁 1 views

Low-temperature (120 K) studies of the structure of the DMAN Á DCI adduct indicate that in symmetrical [NHN] hydrogen bridge of 2.571 (1) A ˚length (2.579(2) A ˚at room temperature) there is a disorder of the H-atom occupying two positions at nitrogen atoms with a distance of 0.94(3) A ˚. The compa