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1,4-Diaza-bicyclo[2,2,2]octane as a Novel and Efficient Catalyst for the Synthesis of 3,4,6-Trisubstituted 2-Pyridone Derivatives

✍ Scribed by Majid M. Heravi; Leili Tahershamsi; Hossein A. Oskooie; Bita Baghernejad

Publisher: John Wiley and Sons
Year: 2010
Tongue: English
Weight: 49 KB
Volume: 28
Category: Article
ISSN: 0256-7660
DOI: 10.1002/cjoc.201090130

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## Abstract A process for double deuterium labeling of an alcohol was developed. The process was utilized in the subsequent tritium labeling of a secondary alcohol with high specific activity (24 Ci/mmol) by reduction of the corresponding ketone using sodium borotritide. The starting ketone was fir