13C spectra of liquid crystals and nonrigid solids using a high-resolution spectrometer
β Scribed by C.A Fyfe; J.R Lyerla; C.S Yannoni
- Publisher
- Elsevier Science
- Year
- 1978
- Weight
- 257 KB
- Volume
- 31
- Category
- Article
- ISSN
- 0022-2364
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## Abstract The mechanical and electronic design of a βmagic angleβ NMR probe is described. This probe can be incorporated in a conventional small gap ^13^C FT spectrometer, without any hardware or software change, to obtain high resolution ^13^C NMR spectra on organic solids. A simple way of tunin
High-resolution 13 C NMR spectra of Λ,Ο-bis[(4,4 0 -cyanobiphenylyl)oxy]alkanes (CBA-n, n D 7, 9 and 10) were measured in chloroform solution and in the polycrystalline state. The spectra of the samples in solution are essentially the same; in the polycrystalline state, on the other hand, the spectr