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13C-NMR Spectroscopy of Keratan Sulphates : Assignments for Four Poly(N -Acetyllactosamine)-Repeat-Sequence Tetrasaccharides Derived from Bovine Articular Cartilage Keratan Sulphate by Keratanase II Digestion

✍ Scribed by Thomas N. Huckerby; Gavin M. Brown; Ian A. Nieduszynski

Book ID: 115131369
Publisher: John Wiley and Sons
Year: 1995
Tongue: English
Weight: 527 KB
Volume: 231
Category: Article
ISSN: 1432-1327
DOI: 10.1111/j.1432-1033.1995.0779d.x

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## Abstract A full assignment of the 60°C ^13^C NMR spectrum for the reduced form of a repeat unit β‐linked tetrasaccharide derived by keratanase digestion from keratan sulphate, GlcNAc(6SO~4~)β^1–3^Gal(6SO~4~)β^1–4^GlcNAc(6SO~4~)β^1–3^‐Gal‐ol, was achieved via two‐dimensional C/H correlation and ^