The 13C NMR signals for some 4substituted phenacyl bromides were assigned. The experimental chemical shifts of the aromatic ring carbons are in close agreement with those calculated using substituent chemical shifts. Both the car-bony1 and the a-methylene carbons exhibit upfield shifts compared with
13C NMR spectra of some 4-substituted protoadamantanes
✍ Scribed by S. E. Morgan; D. M. Rackham
- Publisher
- John Wiley and Sons
- Year
- 1981
- Tongue
- English
- Weight
- 274 KB
- Volume
- 16
- Category
- Article
- ISSN
- 0749-1581
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✦ Synopsis
Abstract
The ^13^C NMR spectra of some mono‐ and geminal disubstituted protoadamantanes have been assigned with the aid of shift reagents.
📜 SIMILAR VOLUMES
The positions of the chemical shifts in the table match those of the carbon atoms at the head of a column. Assignments with similar chemical shifts may be interchanged. Fourth signal not resolved. Signals superimposed.
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## Abstract ^13^C NMR data for 21 cycloalkanespiro‐hydantoin derivatives, substituted at position 3, are reported and compared with those for the corresponding 4‐hydroxy derivatives.
## Abstract ^1^H and ^13^C NMR spectra of 22 2‐substituted 4,5‐dimethylfurans are reported. The __J__(C, H) values were used for signal assignments and for the identification of geometrical isomers of some derivatives.
## Abstract ^13^C chemical shifts for 16 derivatives of furo[3,2‐__b__] pyrrole substituted at positions 2, 4 and 5 are reported. The __J__(CH) values were determined for some derivatives. Heterocorrelated 2D ^1^H‐^13^C NMR spectra, selective heteronuclear decoupling and selective INEPT experiments