## Abstract ^29^Si and ^13^C NMR chemical shifts are reported for __tert__‐butyldimethylsilyl (TBDMS) derivatives of ten common amino acids. The ^29^Si chemical shifts of TBDMS derivatives of various functionalities encountered fall into distinct spectral regions. The ^29^Si chemical shifts correla
13C NMR chemical shifts of ω-haloalkyl-trimethylsilyl and -tert-butyldimethylsilyl ethers
✍ Scribed by Helmut Poleschner; Matthias Heydenreich
- Publisher
- John Wiley and Sons
- Year
- 1991
- Tongue
- English
- Weight
- 174 KB
- Volume
- 29
- Category
- Article
- ISSN
- 0749-1581
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✦ Synopsis
Abstract
The ^13^C NMR chemical shifts of Me~3~SiO(CH~2~)~n~(1, X = I, n = 2–6, 8, 10; 2, X = Br, n = 2, 4, 6, 8, 10; 3, X = Cl, n = 2, 4, 6; 4, X = F, n = 6) and t‐BuMe~2~SiO(CH~2~)~n~(5, X = I, n = 2–4; 6, X = Cl, n = 4) are presented and assigned.
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