In the title compound, C~13~H~14~N~2~O~3~, the morpholine ring adopts the usual chair conformation. The crystal structure is stabilized by weak CβH...O hydrogen-bond interactions.
1,3,4,10b-Tetrahydro-4-phenylpyrido[2,1-a]isoindole-2,6-dione
β Scribed by Beckwith, A. L. J. ;Joseph, S. P. ;Mayadunne, R. T. A. ;Willis, A. C.
- Book ID
- 114511912
- Publisher
- International Union of Crystallography
- Year
- 1995
- Tongue
- English
- Weight
- 345 KB
- Volume
- 51
- Category
- Article
- ISSN
- 0108-2701
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SociM suisse de chimie, Bale -Societ& svizzera di chimica, Basilea Nachdruck verboten -Tous droits reserv6s -Printed by Birkhauser AG.
An efficient synthesis of novel spiro 2,3,7,8-tetrahydro-benzo[1,2-b:5,4-b 0 ]dipyran-4,6-dione and 2,3,8,9tetrahydro-benzo[1,2-b:4,3-b 0 ]dipyran-4,10-dione derivatives in high yields under microwave irradiation is described. The reaction was also studied under conventional heating conditions.
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In the title compound, C 16 H 13 Cl 3 N 2 O 3 S, the 1,3-thiazole ring is almost orthogonal to the isoindoline plane, making a dihedral angle of 89.74 (9) . Intermolecular O-HΓ Γ ΓN and C-HΓ Γ ΓO interactions and SΓ Γ ΓO short contacts link the molecules into a three-dimensional framework. The cryst