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1,3-dipolar cycloaddition reaction: Synthesis and configuration of norcantharidin derivatives of substituted aromatic amine

โœ Scribed by Liping Deng; Yongzhou Hu

Publisher
Journal of Heterocyclic Chemistry
Year
2007
Tongue
English
Weight
416 KB
Volume
44
Category
Article
ISSN
0022-152X

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โœฆ Synopsis

Abstract

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A series of eighteen novel compounds that have potential pharmacological properties has been synthesized by 1,3โ€dipolar cycloaddition reactions of 5,6โ€dehydronorcantharidin derivatives of substituted aromatic amine with nitrile oxide. The synthesis was carried out following straightforward threeโ€step procedure described herein. IR, ^1^H nmr and ms, Hโ€H cosy and Noesy Cyclonoe, confirmed the structure of all products respectively. The biological evaluation of three series of norcantharidin analogues against HL60 cell has been screened.

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## Abstract magnified image Highly efficient, practical and convient synthesis of fifteen compounds by the [3+2] 1,3โ€dipolar cycloaddition reaction of norcantharidin derivatives of substituted aromatic amines with three hydrazines in the presence of Chloramineโ€T.