𝔖 Bobbio Scriptorium
✦   LIBER   ✦

1,2,3,4-Tetra-O-acetyl-α-d-gluco­pyran­uron­amide

✍ Scribed by Baddeley, Thomas C. ;Davidson, Iain G. ;Skakle, Janet M. S. ;Wardell, James L.

Publisher
International Union of Crystallography
Year
2002
Tongue
English
Weight
277 KB
Volume
58
Category
Article
ISSN
1600-5368

No coin nor oath required. For personal study only.

✦ Synopsis

The title compound, C 14 H 19 NO 10 , forms strong hydrogen bonds via amido groups in the [100] direction; soft CÐHÁ Á ÁO bonds also act to give chains along both [100] and [001], which combine to form a two-dimensional layer.

📜 SIMILAR VOLUMES

Prop-2-ynyl 1,2,3,4-tetra-O-acetyl-β-d-g
Prop-2-ynyl 1,2,3,4-tetra-O-acetyl-β-d-gluco­pyran­uronate
✍ Temelkoff, David P. ;Norris, Peter ;Zeller, Matthias 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 495 KB

Single-crystal X-ray study T = 100 K Mean '(C±C) = 0.003 A Ê R factor = 0.043 wR factor = 0.106 Data-to-parameter ratio = 9.4 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

2,3,4,6-Tetra-O-acetyl-β-d-gluco­pyran­o
2,3,4,6-Tetra-O-acetyl-β-d-gluco­pyran­osyl azide
✍ Temelkoff, David P. ;Norris, Peter ;Zeller, Matthias 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 246 KB

The structure of the title compound, C 14 H 19 N 3 O 9 , has been determined at 100 K. The six-membered ring exhibits a chair conformation, and all non-H substituents are found in equatorial positions.