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1,2,3-triazol-1-imines. 2. Electric dipole moments and semiempirical studies of some 2-aryl-N-benzoyl-4,5-dimethyl-1,2,3-triazol-1-imines

✍ Scribed by C. P. Hadjiantoniou-Maroulis; P. D. Akrivos; A. J. Maroulis

Book ID
112130734
Publisher
Journal of Heterocyclic Chemistry
Year
1993
Tongue
English
Weight
224 KB
Volume
30
Category
Article
ISSN
0022-152X

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1,2,3-Triazol-1-imines. Part 3: Tandem 1
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The tandem 1,3 cycloaddition-rearrangement and open chain reactions of 2-aryl-N-aroyl-4,5-dimethyl-1,2,3-triazol-1-imines with DMAD at room temperature and in refluxing toluene are described.

Syntheses of 1-(4-methylsulfonylphenyl)-
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Condensation of 4-methylsulfonylaniline with aryl aldehyde in ethanol-tetrahydrofuran afforded the imino compound 3. 1,3-Cycloaddtion of diazomethane with compound 3 followed by oxidazation of the triazoline 4 with potassium permanganate gave 1-(4-methylsulfonylphenyl)-5-aryl-1,2,3-triazoles 5. Simi