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1',2'-Secothymidines. The preparation of 2,3'-anhydro derivatives and the formation of two unusual dimeric products

✍ Scribed by Cichy, Anne F.; Saibaba, Racha; El Subbagh, Hussein I.; Panzica, Raymond P.; Abushanab, Elie

Book ID
126219746
Publisher
American Chemical Society
Year
1991
Tongue
English
Weight
893 KB
Volume
56
Category
Article
ISSN
0022-3263

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Table 3. C')cloaddirion of allylsilane 2b and methyl propynoate (13) Reaction conditions 14. Yield [%I 15, Yield [%I 3 equiv 2b. -7X C --20 C. 19 h 4equi\2h. -78 t -2 5 C . 5 d 45 46 [a] 98 -3 e q u i v Z h . X C -4 0 C . 1 9 h 34 64 [a] [a] ( i i i r r . \ i +IS: \ w , . \ j ~i i -l S = 3: 1. Trace