𝔖 Bobbio Scriptorium
✦   LIBER   ✦

1,2-Dibromo-4,5-dimethylbenzene

✍ Scribed by Li, Yinhuai

Book ID
104491678
Publisher
International Union of Crystallography
Year
2007
Tongue
English
Weight
783 KB
Volume
63
Category
Article
ISSN
1600-5368

No coin nor oath required. For personal study only.

✦ Synopsis

In the title compound, C 8 H 8 Br 2 , the bond lengths and angles are in the normal range. All non-H atoms are coplanar.

Related literature

The structures of the related compounds 1,2-dibromo-4,5dimethyl-3-nitrobenzene and 1,2-dibromo-4,5,6-trimethyl-3nitrobenzene have been reported by Skakle et al. (2006). For related literature, see: Allen et al. (1987); Lawson et al. (1968); Stoddart (1989). Experimental Crystal data C 8 H 8 Br 2 M r = 263.96 Monoclinic, P2 1 =n a = 9.383 (4) A b = 7.918 (3) A c = 12.612 (5) A = 109.041 (6) V = 885.7 (6) A ˚3 Z = 4 Mo K radiation = 9.08 mm À1 T = 298 (2) K 0.20 Â 0.12 Â 0.10 mm Data collection Bruker SMART CCD diffractometer Absorption correction: multi-scan (SADABS; Sheldrick, 1996) T min = 0.264, T max = 0.464 (expected range = 0.230-0.403) 4542 measured reflections 1735 independent reflections 1346 reflections with I > 2(I) R int = 0.024 Refinement R[F 2 > 2(F 2 )] = 0.036 wR(F 2

📜 SIMILAR VOLUMES

Triethyl­ammonium di­chloro­[1,2-bis(2-p
Triethyl­ammonium di­chloro­[1,2-bis(2-pyridine­carbox­amido)-4,5-di­methyl­benzene]­ferrate(III)
✍ Lee, Sung Jea ;Lee, Jun Yong ;Kim, Cheal ;Nam, Wonwoo ;Kim, Youngmee 📂 Article 📅 2002 🏛 International Union of Crystallography 🌐 English ⚖ 198 KB

Single-crystal X-ray study T = 298 K Mean '(C±C) = 0.004 A Ê R factor = 0.040 wR factor = 0.120 Data-to-parameter ratio = 16.0 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

Crystallographic report: [(Pyridine)(1,2
Crystallographic report: [(Pyridine)(1,2-bis(2-pyrazinecarboxamido)-4,5-dimethylbenzene)zinc(II)] monohydrate
✍ Ji Young Ryu; Jun Yong Lee; Jin Soo Seo; Cheal Kim; Youngmee Kim 📂 Article 📅 2003 🏛 John Wiley and Sons 🌐 English ⚖ 72 KB 👁 1 views

## Abstract The N~4~ donor ligand, Me~2~bpzb^2−^ and a pyridine molecule are coordinated to the Zinc(II) so that the coordination geometry closely resembles a square‐pyramidal environment with a nitrogen atom of the pyridine ligand occupying the apical position. Copyright © 2003 John Wiley & Sons,