119Sn solid-state NMR as a local probe for correlations in
✍ Scribed by E.M. Brüning; M. Baenitz; A.A. Gippius; S. Paschen; A.M. Strydom; F. Steglich
- Publisher
- Elsevier Science
- Year
- 2006
- Tongue
- English
- Weight
- 125 KB
- Volume
- 378-380
- Category
- Article
- ISSN
- 0921-4526
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## Abstract To allow for single‐crystal nuclear magnetic resonance (scNMR) investigations, an existing narrow bore high‐field double‐resonance millicoil ^19^F and ^1^H solid‐state NMR probe was modified by adding a goniometer stage to the top. The goniometer was kept outside of the radiofrequency (
## Abstract A simple method is reported for temperature calibration of a magic angle spinning probe for solid‐state NMR spectroscopy. The method is an extension of that developed by van Geet for temperature calibration of liquid‐state NMR probes, and consists of measuring the frequency difference (