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119Sn-NMR-spektroskopische Untersuchungen an Tri-n-butylzinnderivaten von N-Acetylaminosäuren

✍ Scribed by Jens Klein; Frank Thunecke; Rolf Borsdorf

Publisher
Springer Vienna
Year
1992
Tongue
English
Weight
426 KB
Volume
123
Category
Article
ISSN
0026-9247

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An efficient method for the deuteration of N-acetyl-D-neuraninicacid (NeuAc) at C-3 is described. In alkaline D20 solution both protons of NeuAc (H3a and H3e) will be substituted by deuterium, whereby the substitution effect was found to be faster for H3a than for H3e . The rate of this exchange dep