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10-(4-Methoxy­phen­yl)-3,7-dimethyl-1H,9H,10H-dipyrano[3,4-e:4′,3′-b]pyran-1,9-dione

✍ Scribed by Gao, Yuan ;Zhang, Yan ;Tu, Shujiang


Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
123 KB
Volume
62
Category
Article
ISSN
1600-5368

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✦ Synopsis


The title compound, C 20 H 16 O 6 , was synthesized by the reaction of 4-methoxybenzaldehyde with triacetic acid lactone in ethylene glycol catalyzed by KF-alumina. The pyran ring adopts a boat conformation and the benzene ring is perpendicular to the mean plane through the fused ring system.


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10-(4-Chlorophenyl)-9-(4-methoxyphenyl)-
✍ Chen, Yan ;Hao, Wen-Juan ;Tang, Zi-Qiang ;Jiang, Bo ;Li, Chun-Mei 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 833 KB

The title compound, C 30 H 32 ClNO 3 , was synthesized by the reaction of dimedone with 4-methoxybenzaldehyde and 4chlorobenzenamine in water. The dihydropyridine ring is in a boat conformation. Both cyclohexene rings adopt envelope conformations. The chlorophenyl and methoxyphenyl rings form dihedr