The title compound, C 27 H 24 N 2 O 4 , has been synthesized by the reaction of 4-nitrobenzaldehyde, 3-(cyclopropylamino)-5,5dimethylcyclohex-2-enone and 1,3-indanedione in a mixed solvent of ethylene glycol and acetic acid under microwave irradiation. The dihydropyridine ring adopts a boat conforma
10-(2-Bromo-4,5-dimethoxybenzyl)-7-chloro-5-cyclopropyl-9-methyl-5,10-dihydro-4,5,6,10-tetraazadibenzo[a,d]cyclohepten-11-one
✍ Scribed by Sarala, G. ;Thimme Gowda, N. R. ;Rangappa, K. S. ;Sridhar, M. A. ;Shashidhara Prasad, J.
- Publisher
- International Union of Crystallography
- Year
- 2006
- Tongue
- English
- Weight
- 127 KB
- Volume
- 62
- Category
- Article
- ISSN
- 1600-5368
No coin nor oath required. For personal study only.
✦ Synopsis
In the crystal structure of the title compound, C 24 H 22 BrCl-N 4 O 3 , there are C-HÁ Á ÁO and C-HÁ Á ÁBr intermolecular hydrogen bonds, and also C-HÁ Á ÁO, C-HÁ Á ÁBr and C-HÁ Á ÁN intramolecular hydrogen bonds.
📜 SIMILAR VOLUMES
3-(4-Chlorophenyl)-5-methyl-2-propylamino-8,9,10,11-tetrahydro-2-benzothieno[2 0 0 0 ,3 0 0 0 ;2,3]pyrido [4,5-d]pyrimidin-4(3H)-one
Two molecules of the title compound are related by a twofold non-crystallographic symmetry operation. There is an extensive hydrogen-bonding network, as well as van der Waals interactions between alkyl groups.