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1-Chloro­acetyl-2,4-di­phenyl-2,3-di­hydro-1H-1,5-benzodiazepine

✍ Scribed by Low, John Nicolson ;Cobo, Justo ;Insuasty, Braulio ;Insuasty, Henry ;Díaz, Emilso ;Escobar, Henry


Publisher
International Union of Crystallography
Year
2003
Tongue
English
Weight
363 KB
Volume
59
Category
Article
ISSN
1600-5368

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✦ Synopsis


Single-crystal X-ray study T = 120 K Mean '(C±C) = 0.007 A Ê Disorder in solvent or counterion R factor = 0.068 wR factor = 0.201 Data-to-parameter ratio = 15.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.


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3-(4-Chloro­phenyl)-3,4-di­hydro­quinazo
✍ Shi, Daqing ;Li, Zhengyi ;Shi, Chunling ;Wang, Xiangshan ;Zhang, Yong 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 294 KB

The title compound, C 14 H 11 ClN 2 O, was synthesized by the reaction of N-(4-chlorophenyl)-2-nitrobenzylamine with triphosgene, induced by a low-valent titanium reagent (TiCl 4 /Zn). The dihydroquinazoline ring adopts a skew-boat conformation.