1-Chloroacetyl-2,4-diphenyl-2,3-dihydro-1H-1,5-benzodiazepine
✍ Scribed by Low, John Nicolson ;Cobo, Justo ;Insuasty, Braulio ;Insuasty, Henry ;Díaz, Emilso ;Escobar, Henry
- Publisher
- International Union of Crystallography
- Year
- 2003
- Tongue
- English
- Weight
- 363 KB
- Volume
- 59
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
Single-crystal X-ray study T = 120 K Mean '(C±C) = 0.007 A Ê Disorder in solvent or counterion R factor = 0.068 wR factor = 0.201 Data-to-parameter ratio = 15.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
📜 SIMILAR VOLUMES
The title compound, C 14 H 11 ClN 2 O, was synthesized by the reaction of N-(4-chlorophenyl)-2-nitrobenzylamine with triphosgene, induced by a low-valent titanium reagent (TiCl 4 /Zn). The dihydroquinazoline ring adopts a skew-boat conformation.