1-Benzyl-5-(1-naphthylmethylene)piperidinespiro-3,3′-1′-methyl-4′-(1-naphthyl)pyrrolidinespiro-2′,3′′-indole-2′′,4-dione–diethyl ether (1/0.75)
✍ Scribed by Li, Xiao-Fang ;Feng, Ya-Qing ;Hu, Xiao-Fen ;Wang, Guan
- Book ID
- 104480599
- Publisher
- International Union of Crystallography
- Year
- 2003
- Tongue
- English
- Weight
- 211 KB
- Volume
- 59
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.005 A Ê Disorder in solvent or counterion R factor = 0.062 wR factor = 0.188 Data-to-parameter ratio = 13.3
For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
📜 SIMILAR VOLUMES
In the title compound, C 27 H 21 N 3 , the tetrahydrobenzene ring adopts a half-chair conformation. The orientations of the attached phenyl and tricyanophenyl substituents are determined by the sp 3 state of the tetrahydrobenzene atoms.
Single-crystal X-ray study T = 173 K Mean '(C±C) = 0.009 A Ê Some non-H atoms missing Disorder in solvent or counterion R factor = 0.134 wR factor = 0.363 Data-to-parameter ratio = 26.1 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/