1-[5-Acetyl-2,6-dimethyl-4-(5-phenyl-1 H -pyrazol-3-yl)-1,4-dihydropyridin-3-yl]ethanone monohydrate
✍ Scribed by Islor, Arun M.; Malladi, Shridhar; Sundershan, S.; Gerber, Thomas; Hosten, Eric; Betz, Richard
- Book ID
- 120208785
- Publisher
- International Union of Crystallography
- Year
- 2012
- Tongue
- English
- Weight
- 810 KB
- Volume
- 68
- Category
- Article
- ISSN
- 1600-5368
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📜 SIMILAR VOLUMES
The title compound, C 18 H 18 N 2 O, was prepared by the reaction of 3-phenyl-1-(p-tolyl)prop-2-en-1-one with hydrazine hydrate in acetic acid. The pyrazole ring is in an envelope conformation. The crystal packing is stabilized by van der Waals forces.
The title compound, C 27 H 16 Cl 2 F 6 N 4 O 2 ÁH 2 O, was obtained by the reaction of 2,4-dichlorobenzaldehyde and 2-phenyl-5trifluoromethyl-2H-pyrazol-3-ol in aqueous media without any catalyst. In the crystal structure, both intra-and intermolecular hydrogen bonds are found.
In the title compound, C 13 H 12 N 4 OÁH 2 O, NÁ Á ÁH-O and OÁ Á ÁH-O hydrogen bonds involving the uncoordinated water molecules link the molecules into two-dimensional networks parallel to the (101) planes.