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1-[2,6-Dichloro-4-(trifluoro­methyl)phenyl]-5-[(dimethyl­sulfonyl)amino]-1H-pyrazole-3-carbonitrile

✍ Scribed by Yang, Zhi-Ping ;Zhong, Ping ;Hu, Mao-Lin ;Li, Shu-Yan ;Tang, Ri-Yuan

Publisher
International Union of Crystallography
Year
2004
Tongue
English
Weight
390 KB
Volume
61
Category
Article
ISSN
1600-5368

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✦ Synopsis

Single-crystal X-ray study T = 298 K Mean '(C±C) = 0.005 A Ê R factor = 0.049 wR factor = 0.135 Data-to-parameter ratio = 13.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

📜 SIMILAR VOLUMES

1-[2,6-Di­chloro-4-(tri­fluoro­methyl)­p
1-[2,6-Di­chloro-4-(tri­fluoro­methyl)­phenyl]-5-[(4-methyl­benzyl­idene)­amino]-1H-pyrazole-3-carbo­nitrile
✍ Zhong, Ping ;Yang, Zhiping ;Shi, Qian ;Li, Shuyan ;Tang, Riyuan 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 75 KB

Single-crystal X-ray study T = 298 K Mean (C±C) = 0.005 A Ê Disorder in main residue R factor = 0.072 wR factor = 0.215 Data-to-parameter ratio = 13.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

1-[2,6-Di­chloro-4-(tri­fluoro­methyl)­p
1-[2,6-Di­chloro-4-(tri­fluoro­methyl)­phenyl]-5-[(4-di­methyl­amino­benzyl­idene)­amino]-1H-pyrazole-3-carbo­nitrile
✍ Chen, Dimei ;Yang, Zhiping ;Zhong, Ping ;Hu, Maolin 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 60 KB

The title compound, C 20 H 14 Cl 2 F 3 N 5 , is a tricyclic amide with an overall U-shape, each of the the three rings being planar. There areinteractions between the pyrazole ring and the benzene ring with the dimethylamine substituent.

5-Amino-4-chloro-1-[2,6-dichloro-4-(trif
5-Amino-4-chloro-1-[2,6-dichloro-4-(trifluoro­meth­yl)phen­yl]-1H-pyrazole-3-carbonitrile
✍ Li, Shu-Yan ;Zhong, Ping ;Hu, Mao-Lin ;Li, Jin-Hai 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 209 KB

In the title compound, C~11~H~4~Cl~3~F~3~N~4~, the dihedral angle between the pyrazole and the N-substituted benzene ring planes is 84.5 (2)°. The crystal structure is stabilized by N—H...N hydrogen bonds.