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1-[2,6-Di­chloro-4-(tri­fluoro­methyl)­phenyl]-5-(2,5-dioxo-2,5-di­hydro-1H-pyrrol-1-yl)-1H-pyrazole-3-carbo­nitrile

✍ Scribed by Yang, Zhiping ;Zhong, Ping ;Hu, Maolin

Publisher
International Union of Crystallography
Year
2004
Tongue
English
Weight
292 KB
Volume
60
Category
Article
ISSN
1600-5368

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✦ Synopsis

Single-crystal X-ray study T = 298 K Mean '(C±C) = 0.004 A Ê R factor = 0.055 wR factor = 0.165 Data-to-parameter ratio = 13.7

For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

📜 SIMILAR VOLUMES

5-(2-Chloro­benz­amido)-1-[2,6-di­chloro
5-(2-Chloro­benz­amido)-1-[2,6-di­chloro-4-(tri­fluoro­methyl)­phenyl]-1H-pyrazole-3-carbo­nitrile
✍ Zhang, Xiao-Hong ;Zhong, Ping ;Yang, Zhi-Ping ;Hu, Mao-Lin ;Xiao, Hong-Ping 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 227 KB

The molecule of the title compound, C 18 H 8 Cl 3 F 3 N 4 O, is a tricyclic amide with an overall U-shape. Intermolecular N-HÁ Á ÁN hydrogen bonds, with an N(amide)Á Á ÁN(cyano) separation of 3.051 (4) A ˚, link the molecules into linear chains along the c axis.

1-[2,6-Di­chloro-4-(tri­fluoro­methyl)­p
1-[2,6-Di­chloro-4-(tri­fluoro­methyl)­phenyl]-5-[(4-methyl­benzyl­idene)­amino]-1H-pyrazole-3-carbo­nitrile
✍ Zhong, Ping ;Yang, Zhiping ;Shi, Qian ;Li, Shuyan ;Tang, Riyuan 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 75 KB

Single-crystal X-ray study T = 298 K Mean (C±C) = 0.005 A Ê Disorder in main residue R factor = 0.072 wR factor = 0.215 Data-to-parameter ratio = 13.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

1-[2,6-Di­chloro-4-(tri­fluoro­methyl)­p
1-[2,6-Di­chloro-4-(tri­fluoro­methyl)­phenyl]-5-[(4-di­methyl­amino­benzyl­idene)­amino]-1H-pyrazole-3-carbo­nitrile
✍ Chen, Dimei ;Yang, Zhiping ;Zhong, Ping ;Hu, Maolin 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 60 KB

The title compound, C 20 H 14 Cl 2 F 3 N 5 , is a tricyclic amide with an overall U-shape, each of the the three rings being planar. There areinteractions between the pyrazole ring and the benzene ring with the dimethylamine substituent.