𝔖 Bobbio Scriptorium
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1-(1-Benzofuran-2-yl)-2-chloroethanone

✍ Scribed by Kozakiewicz, Anna ;Prewysz-Kwinto, Andrzej ;Wojtczak, Andrzej

Publisher
International Union of Crystallography
Year
2007
Tongue
English
Weight
531 KB
Volume
63
Category
Article
ISSN
1600-5368

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✦ Synopsis

The title compound, C 10 H 7 ClO 2 , was synthesized from 1-benzofuran-2-ylethanone by chlorination with thionyl chloride. The benzofuran ring system and the carbonyl group are coplanar. The carbonyl group is in a syn position relative to both the O atom of the benzofuran ring and the Cl atom. C-HÁ Á ÁO contacts are found between the methylene group and carbonyl O atom. Molecules related by a centre of symmetry are involved ininteractions, with distances between the centroids of the furan rings of 3.785 (3) A ˚.

📜 SIMILAR VOLUMES

1-(1-Benzo­furan-2-yl)-2-mesityl­ethano­
1-(1-Benzo­furan-2-yl)-2-mesityl­ethano­ne
✍ Arıcı, Cengiz ;Ülkü, Dinçer ;Kırılmış, Cumhur ;Koca, Murat ;Ahmedzade, Misir 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 389 KB

Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.005 A Ê R factor = 0.058 wR factor = 0.154 Data-to-parameter ratio = 12.9 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

1-(3-Amino-1-benzo­furan-2-yl)-2-mesityl
1-(3-Amino-1-benzo­furan-2-yl)-2-mesityl­ethano­ne
✍ Arıcı, Cengiz ;Ülkü, Dinçer ;Kırılmış, Cumhur ;Koca, Murat ;Ahmedzade, Misir 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 277 KB

Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.005 A Ê R factor = 0.054 wR factor = 0.132 Data-to-parameter ratio = 11.9 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

2-(5-Ethyl-3-methylsulfanyl-1-benzofuran
2-(5-Ethyl-3-methylsulfanyl-1-benzofuran-2-yl)acetic acid
✍ Seo, Pil Ja ;Choi, Hong Dae ;Son, Byeng Wha ;Lee, Uk 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 161 KB

The title compound, C 13 H 14 O 3 S, was prepared by alkaline hydrolysis of ethyl 2-(5-ethyl-3-methylsulfanyl-1-benzofuran-2-yl)acetate. The crystal structure is stabilized by aromaticstacking interactions and inversion-related intermolecular O-HÁ Á ÁO hydrogen bonds between adjacent carboxyl groups